Materials Characterization application examples
MeTiS: Characterization of inclusion population
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MeTiS : software application for automatic characterization of inclusion population in the metallurgical industry
MeTiS was developed by Datamet to characterize inclusion population automatically from images from an optical microscope or a system consisting of a scanning electron microscope and EDS analyzer.
The benefits of Metis Measure are:
Examples of inclusions detected
Processing software, dissociated measurement software allows multiple operations data measurement files, and return the results in Microsoft Excel.
The main specificities of MeTis are:
The benefits of MeTis Treatment are :
The simulation software provides access to statistical parameters of the various methods by measures calculated on virtual samples.
The advantages of MetiS Simulation are :
An article describing the application is published in the journal JEOL News in July 2006.
Version for optical microscopy
MeTiS version for optical microscopy offers the same features as the version for electron microscopy, with the exception of the following features:
Automatic study of Ceramics material
Development of a vertical application for the study of ceramics
ADCIS and the LERMAT, a research laboratory specialized in Material Science jointly developed automatic tools to analyze ceramics using Image Processing techniques. During the course of this 2 year project, two types of ceramics were analyzed, a ceric oxide, used for sintered analysis, and alumine-zircone, a two phase material used for grain detection and analysis.
A scanning electron microscope was used to acquire black and white, very high resolution images. Some filtering operators were applied to the images to enhance their quality by removing visible noise. Segmentation of the images involved automatic thresholding techniques to detect grains and pores, and various morphological operators such as top-hat, skeleton by zone of influence, watershed with constrained markers, and other functions looking at the size distribution of particles.
The images below present an example of image processing algorithms applied to a ceric oxide sintered at a temperature of 1200 degrees during a 5 hour process.
The research work also involved an in-depth analysis of the sample to measure characteristics such as granulometry, evolution of the volumic fraction versus the temperature, kinetics laws, pore dispersion, etc. The following chart displays the evolution of the granulometry.
Finally, some probabilistic models were studied to determine a model for the micro-structure.
This comprehensive work was performed within the scope of a Ph.D. thesis, and was partially funded by an ITIC grant from the Normandy region in France.
All image processing and analysis functions were developed using Aphelion™ and are now available as a set of macros written in Basic Script.
Grain boundary detection
Grain boundary detection example
This software solves a common problem in materials science, namely the detection of grain boundaries. For example, ASTM standards refer to this detection.
The user interface appears as a combination of several windows with buttons calling some functions of image processing and mathematical morphology. The judicious combination of these features can automatically detect the grains and their boundaries in calling functions segmentation and analysis of size and shape. The user has very few parameters to be specified before the launch detection and the output image of the algorithm contains boundaries thinned and thick one pixel.
This software is absolutely expectations metallurgists who wish to automate the detection of grain material and quantify the number of phases and inclusions in steel. The software is based on a stand-alone program that takes an image in TIFF format as input and generates an image at the same output format. All measurements are exported to a file in Microsoft Excel format. The demo version is an executable Visual Basic.
The advantages of the detection software grain boundaries are:
The algorithm includes edge detection, two types of transformations Top Hat Form to solve the problem of non-uniform illumination, an edge detection, filtering, operations erosion and dilation to clean contours, a line algorithm Watershed and skeleton by influence zone.
Extract volume fraction of zircone grains in aluminum
Below is an application that was developed by an Aphelion™ users in the field of Material Science. The image is courtesy of ESRF Grenoble, INSA de Lyon, GEMPPM, and Ecole des Mines de Paris.
The goal of the application is to extract volume fraction of zircone grains in aluminum, to compute grain sizing and determine neighbor distribution, working on the 3D volume.
In the past, most of the 3D analysis were performed using the set of 2D sections of a 3D volume. Nowadays, thanks the processing power of computers, and the quality of sensors, it is possible to deal directly with 3D images.
Below is the description of a very innovative technique based on 3D Morphology and 3D Image Understanding to compute grain sizing and neighbor distribution, two analysis which can only be performed on the 3D data.
With the help of ObjectSets, the computation is no longer performed on pixels, but on 3D objects. Since objects are already individualized in an ObjectSet, and available as rasters, we perform a dilation on the Objects, with the condition that grains remain individualized even if they overlap after the dilation. The final result gives the number of overlaps for each grain, and is displayed in the standard Aphelion grid as a new attribute. This computation is very quickly performed since no pixel information is required, and it really proves Aphelion has superior capability than any other software when dealing with 3D images.
The following chart gives the neighbor distribution for the Zircone image, and the grid shows the value of the neighbor attribute. As in the 2D version of Aphelion, message passing is available between the grid and the chart.